濟(jì)南聚大邦成化工有限公司
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精萘廠家:提取的方法
精萘的提取可以通過多種方法進(jìn)行,以下是幾種常見的精萘提取方法:
The extraction of refined naphthalene can be carried out through various methods, and the following are several common methods for extracting refined naphthalene:
煤焦油提取法 :
Coal tar extraction method:
從高溫煤焦油中分離出萘油餾分(210-230℃),經(jīng)過洗滌脫酚和精餾分離輕組分,得到工業(yè)萘。
Separate naphthalene oil fraction (210-230 ℃) from high-temperature coal tar, wash and dephenolate, and separate light components by distillation to obtain industrial naphthalene.
工業(yè)萘進(jìn)一步通過酸洗和蒸餾,硫含量可降至小于0.1%,再通過加氫精制工藝,硫含量可低于0.05%。
Industrial naphthalene can further reduce its sulfur content to less than 0.1% through acid washing and distillation, and then through hydrogenation refining process, its sulfur content can be reduced to less than 0.05%.
結(jié)晶法 :
Crystallization method:
利用不同純度萘的熔點(diǎn)差異,通過分步結(jié)晶和融化操作,高結(jié)晶點(diǎn)萘進(jìn)入成品槽,低純度萘進(jìn)入殘油罐。
By utilizing the melting point differences of different purity naphthalenes, high crystallization point naphthalenes enter the finished product tank and low purity naphthalenes enter the residual oil tank through step-by-step crystallization and melting operations.
在精制工序中,通過閃蒸進(jìn)一步精制制得精萘。
In the refining process, refined naphthalene is further refined by flash evaporation.
溶劑萃取法 :
Solvent extraction method:
使用乙醇對煤焦油進(jìn)行萃取,然后對萃出液減壓蒸餾,得到含萘量較高的固液混合物,經(jīng)過濾抽干得到粗萘。
Ethanol is used to extract coal tar, and then the extracted liquid is subjected to vacuum distillation to obtain a solid-liquid mixture with high naphthalene content. After filtration and dehydration, crude naphthalene is obtained.
水蒸汽蒸餾法 :
Steam distillation method:
建立水蒸汽蒸餾提純粗萘的方法,所得精萘純度可達(dá)99.48%,回收率在93%以上。
Establishing a method for steam distillation purification of crude naphthalene, the purity of refined naphthalene obtained can reach 99.48%, with a recovery rate of over 93%.
分步結(jié)晶法 :
Stepwise crystallization method:
將工業(yè)萘裝入箱式結(jié)晶器中,根據(jù)萘中各餾分結(jié)晶點(diǎn)的差別進(jìn)行分步結(jié)晶提純。
Load industrial naphthalene into a box type crystallizer and perform step-by-step crystallization purification based on the differences in crystallization points of each fraction in naphthalene.
豎管式結(jié)晶法 :
Vertical tube crystallization method:
利用豎管式結(jié)晶器進(jìn)行多級結(jié)晶過程,包括結(jié)晶、發(fā)汗和熔融步驟,生產(chǎn)出高純度的精萘。
Using a vertical tube crystallizer for multi-stage crystallization process, including crystallization, sweating, and melting steps, high-purity refined naphthalene is produced.
反應(yīng)與精餾結(jié)合法 :
Reaction and distillation combined method:
以工業(yè)萘為原料,通過過氧化氫氧化和有機(jī)酸、無機(jī)酸催化,結(jié)合精餾方法提取精萘。
Using industrial naphthalene as raw material, refined naphthalene is extracted through hydrogen peroxide oxidation, organic acid and inorganic acid catalysis, and distillation method.
以上方法中,結(jié)晶法和分步結(jié)晶法因其高純度和節(jié)能效果而被廣泛應(yīng)用。選擇具體提取方法時,需要考慮原料來源、成本、環(huán)境影響及生產(chǎn)規(guī)模等因素。
Among the above methods, crystallization and stepwise crystallization are widely used due to their high purity and energy-saving effects. When selecting a specific extraction method, factors such as raw material sources, costs, environmental impact, and production scale need to be considered.
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This article is provided by the refined naphthalene manufacturer. Our website is: http://m.fkrn12-12.com We will provide you with wholehearted enthusiasm and welcome your visit!
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